Macintosh help Mac OS X Leopard for a non-ejecting disk image problem
Non-ejecting disk image problem of Mac OS X ignores your wish to eject disks and disk images, no matter if you click the Eject button in the Finder’s sidebar, drag the disk to the Trash, or right-click and choose Eject.
Solutions to the non-ejecting disk image problem for Mac OS X
Solution 1: Force Quitting (Relaunching) the Finder (Apple Menu –> Force Quit –> Finder)
Solution 2: open Disk Utility (in the Application->Utilities Folder), and unmount the disk
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